Agilent LVI-PTV-GC/MSDによるpptレベルの半揮発性物質の analysis Manual
Contents
1. AutoSIM AutoSIM 5 2 AutoSIM SIM 156 189 ISTD SS 1 1 1 2 10 SIM 230 250 C2. RT S N SIM 10 50 EPA 525 0 1 10 ppm 1 000 10 0 1 100 ppb RTL GC MSD SIM LVI PTV 2 1
3. 1 GC Agilent 7890A 6890N EPC PTV C min C 20 0 60 1 600 350 1 30 2 10 250 0 00 100 C 10 00 11 77 psi 0 60 100 0 mL min 0 0 psi 50 0 mL min 2 50 53 9 mL min PTV Agilent P N 5183 2037 240V C min C 40 2 50 1 50 110 0 00 2 10 320 1 10 26 0 5 325 C Agilent Technologies HP 5 MSi P N 19091S 433i 30 0 m 0 25 mm 0 25 nm 11 77 psi 1 5 mL min MSD RTL
4. 3 7890A 5975C ppb 0 1 0 0001 ppb 100 0 1 1 25 mL 1 1 mL 1000 1000 1 U S EPA Method 525 2 is available from different sources listed on this Web site www epa gov O WDW methods where html 2 M Szelewski Drinking Water Semivolatiles Analysis Using the 6890N 5975B Inert GC MSD Agilent Technologies publication 5989 5421EN 3 K Weiner N Mata and P Wylie Retention Time Locking with the G1701BA MSD Productivity ChemStation Agilent Technologies publication 5968 3438E 4 M Szelewski B Wilson and P Perkins Improvemenrnts in the Agilent 6890 5973 GC MSD System for Use with U S EPA Method 8270 Agilent Technologies publication 5988 3072EN 5 H Prest and D Peterson New Approaches to the Development of GC MS Selected 1on Moni toring Acquisition and Quantitation Methods Agilent Technologies publication 5988 4188 6 M Szelewski Synchronous SIM Scan Low Level PAH Analysis Using the Agilent Techmologies 6890 5975 Imert GC MSD Agilent Technologies publication 5989 4184EN
5. 100 C RRF RSD RSD RRF GC MSD ChemStation Excel RSD RSD 2 S N RT 7 01 109 8 90 127 12 24 201 12 35 200 12 48 266 14 78 197 2 2 3 4 6 15555 326 16 30 303 pp DDT 18 00 235 SIM Scan
6. p p DDT RSD 9 pp DDD pjp DDE RSD 6 4 p p DDT EPA p p DDT 1 2 1 9 15 S N 2 to PCP 5 S N PCP 3 100 ppt
7. 12 700 d10 GC MSD RTL 3 RTL SIM GC RTL RTL www agilent com chem jp RTL SIM 3 mm 6 mm 4
8. 6 mm S N 6 mm Agilent G2860A SIM 1 SIM SIM Scan 5975C 1 S N 45 450 10 SIM Scan SIM 2
9. 0 01 0 02 0 1 0 1 25 25 1 0 25 10 1 25 www adgilent com chem jp wwwragilent com chem jp Agilent Technologies Inc 2007 Printed in Japan April 13 2007 5989 6589JAJP Agilent Technologies
10. 39 8 C 100 mL min 0O psi 11 77 psi PTV 350 C 1 3 50 mL min PTV PTV PTV GC 1 PTV
11. S N 3 1 L 1 mL 1 nuL 100 ppb 0 1 ppm 7890A 5975C 1 000 ppt 10 mL PCP S N 22 266 100 ppt T T 12 2 11 8 12 0 12 4 12 6 S N 2 7 197 100 ppt ED OE i EE EE El EL I i ES EE EE EN TE EN EL i 0 EE 0 EE EN ES ES EE EE ES EE El EE EE EE a TE EE EE i EE EE ES a EE EE EE DS FE EE EN ES a 14 4 14 6 14 8 15 0 15 2 15 4 3 PCP 10 10 mL
12. 50 ppb 108 3 ISTD 4 SS 1 PTV PTV 150 100 50 nuL min RT PTV 10 20 30 40 C
13. 300 CO PAH 6 26 0 1 1 0 10 100 ppb 4 SIM Scan 1 0 ppb SIM TIC 2
14. PTV P N 5183 2037 25 uL PTV 1 40 C 110 C 240 V 120 V 1 HP 5MSi HP 5MS 1 5 mL min
15. 1 0 ppb SIM TIC EPA 525 30 RSD RRF RSD 2 PCP OPP RSD PCP 525 OPP RSD SIM 12 S N RSD 100 ppt 6 5 4 7 1 17 4 8 6 20 6 22 24 27 12 12 9 3 2 25 13 9 SS RSD 2 4
16. msec 5 10 10 Ultra Scientific North Kingstown RI P N DWK 5252 4 4 108 50 ppb 3 50 ppb 7890A GC 6890N 320 C 40 C 7 4 3 7890A GC MSD PTV 3 3 PTV 1 PTV PTV 20 C 0 6
17. 50 100 200 300 mL min 0 5 50 nuL min 25 uL 0 6 PTV 100 PTV 2
18. 12 700 d10 0 2 25 50 A 0 B 1 A 2 B 2 1 50 nL min 600 pL min 6 000 uL min 0 0 MSD Agilent Technologies 5975C 6 mm P N G2589 20045 4 45 amu 450 amu 0 1 180 C 300 C 280 C EM 1 247 V MSD SIM AutoSIM 25 1 22 2 45
19. 1 L 2 mL Agilent P N 5182 3454 SIM PTV 100 ppt RTL SIM 7890A
20. 20 40 100 LSE Cij EPA 6 Agilent Technologies 525 2 1 MSD 1 uL PTV 1 nL 25 uL PTV
21. LVI PTV GC MSD 1 1 ppt 7 eSe ee e Mike Szelewski Agilent Technologies Inc 2850 Centerville Road Wilmington DE 19808 USA 1 1 ppt 1 pL LVI PTV SIM MSD
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