Agilent 1290 Infinity LC システムによる塩酸メトクロプラミド製剤中不純物 analysis の生産性向上 Manual
Contents
1. Agilent 1290 Infinity LC 880 bar 100 mm HPLC 4 Agilent 1290 Infinity LC 0 001 w w 0 005 w w 50 250 pg 10 1 50 1 1 de Villiers A Lauer H Szucs R Goodall S Sandra P J Chromatogr A 1113 84 91 2006 2 Gritti F Guiochon G J Chromatogr A 1187 165 179 20082. 2 950 pL 1290 Infinity 10 uL 1290 Infinity LC 1290 Infinity LC 1200 1 7 um 2 1 mm id BEH C18 0 22 mL min 2 0 8 380 bar 0 5
3. 5 mg mL Agilent 1290 Infinity LC G1322A G4220A 1290 Infinity G1311A G1313A G4226A 1290 Infinity G1316A G1316C 1290 Infinity G1315B G4212A 1290 Infinity EP P W HzN 0CHs X 9 Br DN CHs HzN 0CHs 1 4 5 2 EP C Cl COOH 2 4 2 EP H 0 TX_ me OH 3 4 5 N 2 CHs 2 N EP G 0 a 1 HzN 0CHs 4 4 5 N 2 CHs 2
4. www agilent com chem 1290 jp Agilent Technologies Inc 2009 May 15 2009 Publication Number 5990 3981JAJP Agilent Technologies
5. 3 5 um 1A 1B 1290 Infinity 2 1 7 um 3 5 um 2 1 4 1 2 2 6 5 9 Agilent 1290 Infnity LC A 1200 LC 6 X B 1290 Infinity LC mAU ow or 8 10 G LE EET EE L
6. Agilent 1290 Infiniy LC DAD 0 001 w w 1 Agilent Technologies 4 5 LC 2 nm 2 nm LC
7. Agilent 1290 Infinity LC 1200 bar DAD 3 5 um Agilent 1200 LC 1 7 um UHPLC Agilent 1290 Infinity LC 2 I Agilent 1200 HPLC Agilent 1290 Infinity LC 1200 HPLC EP 1
8. S N3 0 005 0 05 w w pg 1 1 0000 450 2 65 0 005 250 7 3 2 0 9999 7 54 1 72 0 005 250 8 6 3 1 0000 1 35 0 95 0 001 50 7 9 4 0 9994 1 77 1 74 NA NA9 NA9 5 1 0000 2 35 2 24 0 001 50 3 6 6 0 9997 3 32 0 93 0 001 50 4 3 7 1 0000 2 42 0 49 0 001 50 5 3 8 1 0000 1 92 0 81 0 001 50 4 5 9 1 0000 3 61 1 42 0 001 50 30 90 01 0 02 0 05 0 1 0 2 0 5 1 6 1 1 25 HPLC Agilent 1290 Infinity LC 1200 LC HPLC 1290 Infiniy LC 150 mm x 3 0 mm 3 5 um 1 7 um 2 1 mm 2 nm
9. 0 22 mL min 0 66 mL min 380 bar 1020 bar 1 2 5 7 8 2A 37 C 32 C 2B 4 5 5 LC 3 1 1070 bar 1000 bar A 0 0 5 1 1 5 B 32 C mAU
10. 8 3 5 LOD 4 LOD 0 001 w w 0 005 w w 50 250 pg 10 1 50 1 mAU 4 3 4 2 A 1 0 0 a 0 5 0 75 1 1 25 1 5 1 75 2 2 25 2 5 2 75 mAU 4 3 2 1 6 3 5 78 9 0 0 5 0 75 1 1 25 1 5 1 75 2 2 25 2 5 2 75 a 0 5 0 75 1 1 25 1 5 1 75 2 2 25 2 5 2 75 4 1 9 LOD 0 001 w w 0 005 w w 3 R RSD LOD
11. EP F 6 H2N OH 5 4 5 N 2 6 CHs 2 EP Al N HsC N ocH3 6 4 2 EP D 0 OCH3 Hs3C N 0CH H 7 4 2 0 0 Ye ol H 8 4 5 2 EP B 0 CI 0CH H 9 4 2 0 0OCH H2N OH 1 1 1200 LC 1290 LC Infiniry 1200 HPLC 0 5 w w 1A 3 5 um XBridge C 18 140 bar 1290 Infinity LC 1290 Infinity LC
12. Gerd Vanhoenacker Frank David Pat Sandra Research Institute for Chromatography Kennedypark 26 B 8500 Kortrijk Belgium Bernd Glatz and Edgar Naegele Adgilent Technologies R amp D and Marketing GmbH amp Co KG Hewlett Packard Str 8 76337 Waldbronn Germany Agilent 1290 Infinity LC Agilent 1290 Infinity LC 1200 HPLC LC Agilent 1290 Infinity LC 1070 bar 880 bar 3 5 HPLC 4
13. 200 175 150 125 100 75 50 1 25 0 o 2 5 ww 3 5 4 4 5 0 0 5 1 1 5 2 Ns 2 5 3 3 5 4 4 5 2 1 9 0 5 w w 2 A BEH C18 150 mm x 2 1 mm 1 7 nm A 0 25 w w B 0 66 mL min 0 16 5 B 0 16 5 16 5 57 5 B 37 C 32 C 0 8 DAD 275 4 nm 400 60 nm 1020 bar 1070 bar 150 mm 100 mm 0 66 mL min 880 bar 3 5 nm 15 5
14. 3 5 3 3 8 1200 LC mAU 1 1204 100 x 80 60 4 5 40 2 20 0 1 1 j 0 0 5 1 1 5 2 2 5 3 3 Agilent 1290 Infinity LC 1 9 0 5 w w 3 Agilent 1290 Infinity LC BEH C18 100 mm x 2 1 mm 1 7 nm A 0 25 w w B 0 66 mL min 0 0 1 5 B 0 1 3 45 5 57 5 B 32 C 1 DAD 275 4 nm 400 60 nm 880 bar 3 3 2 gt 0 999 LOD 0 005 RSD
15. E EL EE 1 1 8 10 7 8 9 12 7 8 4 5 9 X 12 1 Agilent 1200 LC Agilent 1290 Infinity 1 9 0 5 w w 1 A XBridge C 18 150 mm x 3 0 mm 3 5 nm BEH C18 150 mm x 2 1 mm 1 7 nm A 0 25 w w B 0 45 mL min 0 22 mL min 0 15 5 57 5 B 0 0 5 5 B 0 5 15 5 5 57 5 B 37 C 37 C 2 0 8 LL DAD 275 4 nm 400 60 nm 140 bar 380 bar 2 Agilent 1290 Infinity LC 1 7 um 380 bar 1290 Infinity LC 1200 bar
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