Agilent LC-(ESI-)-MS/MSによるsub-pptレベルでの水中のエストロン-3-硫酸塩の同定 Manual
Contents
1. E2 E1 E3 EE2 3 3 2002 657 EC 1 10ng d 2 0 45 hm 3 MM4 SPE lg 6mL Imterchim 4 12mL MeOH NH4OH2. d IS 368 3 353 3 A 3 2 349 2 gt 145 2 A L 3 1 LETT TDL TY oo ww eo i 0 w a w JILIIIIIIII 349 2 269 2 MR TIWWI 57 1 1 N RR 97 MM PH 3 55 87 sm9 at 93 55 7 RR 93 55 7 59 PRMU 95 97 99 05ppt 1 IS 2 IS 4 1 0 3 0 8 M AA 0 1 a 2 A J NK y 0 67x 0 22 NK n4 y 0 17x 0 06 R2 0 99 HH R2 0 98 1 n 0 0 0 1 2 3 4 5 6 0 1 2 3 4 5 6 ppt ppt 1 3 5 5 1 2 3 4 5ppt
3. 2 Agilent Technologies Inc 2008 Printed in Japan June 24 2008 5989 8480JAJP Agilent Technologies
4. 368 3 Wide 353 3 349 2 Wide 269 2 349 2 Wide 145 2 2002 657 EC sub ppt 1 2 83 4 5ppt 8 5 3 2 d3 1 MRM 1 MS2 Widest Widest Widest ms 200 300 300 120 200 200 15 35 60 x102 ppt 2 MRM 1ppt 2ppt
5. 98 2 Y V 5 6 50uL MeOH HzO 80 20 v v 0 1 2 38 4 5ng L ppt 6 Agilent Technologies LC MS MS Agilent 1200 Gemini 50mm x 2mm 3 nm C18 110 A Phenomenex Extend C18 3 5 um 2 1 x 50mm P N 735700 902 40 C A 25mM pH 9 2 B ACN 0 3mL min 1 MS MS MS B 0 5 0 5 5 15 5 100 18 5 100 21 5 26 5 10 uL Agilent 6410 LC MS ESI 3 500V 40psi 13L min 275 C 2 MS MS ds 3 T1 3 T2 MS1
6. H H CCo CCB 3 n 25 5 5 CCo 3 R 5 ng L 349 2 gt 145 2 0 954 0 977 6 8 22 6 0 08 349 2 269 2 0 976 0 991 3 9 17 2 0 10 2 CCB ng L 0 15 0 53 www agilent com chem jp 2ng L 12 5 pg x102 d IS E 3 349 2 145 2 x102 E 349 2 gt 2692 ET TT TT TT TT 82 84 86 88 9 92 94 96 98 10 8 1 lt CCo 8 2
7. x10 TTTT 84 8 6 A 8 8 TTTTTTTTTTTTTTITTTTT T 9 92 94 96 98 10 8 82 84 86 88 9 92 94 96 98 10 2 0 2ng L ds IS 349 2 145 2 349 2 269 2 8 8 2 84 8 6 88 92 94 9 6 TTTTTT TTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT 98 10 8 82 84 8 6 8 8 10 2 MRM Hi SPE LC MS MS Gemini Phenomenex Agilent 6410 LC MS 3 2002 657 EC wwwr agilent com chemVjp
8. LC ESI MS MS sub ppt 3 e a ht e 9 e Emmanuelle Bichon Soazig Elaudais and Bruno Le Bizec Laboratoire d Etude des R sidus et Contaminants dans les Aliments LABERCA USC INRA 2013 Ecole Nationale V t rinaire de Nantes ENVN BP 50707 44307 Nantes Cedex 3 France SPE LC MS MS 3 sub ppt
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