Agilent 7693A オートサンプラ(ALS) を用いたバイオディーゼル油の標準溶液及びサンプル前処理の自動化 Manual
Contents
1. Agilent 7890A GC 1 GC EN14103 FAME GC GC 1 D6585 Test Method for Determination of Free and Total Glycerine in B 100 Biodiesel Methyl Esters by Gas Chromatography ASTM International 100 Barr Harbor Drive West Conshohocken PA USA 2007 2 EN14105 Fat and Oil Derivatives Fatty Acid Methyl Este2. GC 4 7693A 4 7693A 7693A G4513A 7693A G4513A 7693A G4520A 100 pL PTFE 5183 2042 10 pL PTFE 5181 3354 5 ASTM D6584 EN14105
3. B100 4 4 10 EN14103 5 6 7 EN14103 3 7693A pA 2 800 600 eo 90 ISTD 1 1 200 1 0 5 7 5 10 12 5 15 17 5 20 22 5 25 pA 800 600 200 2 5 7 5 10 12 5 15 17 5 20 22 5 25 pA 800
4. 15 mL 7693A 2 mL 2 mL 10 D6584 7693A 10 EN14105 1 2 mL 1 2 100 mL 1 100 3 10 pL 1 4 10 unL 2 5 10 pL MSTFA 6 1
5. 800 pL n 9 1 10 10 pL 11 1 pL 12 B100 EN14103 3 B100 B100 10 mg 2 mL 7693A 1 10 mg B100 100 pL 2 500 pL 10 mg mL C17 0 n 100 pL 3 1 4
6. 0 5 10 15 20 3 2 B100 A ASTM D6584 B 10 Agilent 7693A Agilent 7890A 1 4 7693A TT ss 4 5 5 5 5 6 6 5 7 0 16 16 5 17 17 5 2 7693A 4 B100
7. 10 pL 5 1 uu 10 6 B100 ASTM D6584 2 5 1 7693A 2 ASTM D6584 rz 0 99 3
8. hy Agilent Technologies B100 GC 2 ASTM D6584 EN14105 B100 2 GC GC Agilent 7693A GGC 3 GC ASTM D6584 EN14105
9. GC B100 Aqgilent 7890A GC 7693A ASTM D6584 EN14105 3 EN14103 B100 FAME B100 7693A Agilent 7890A GC 1 GC EN14103 HP INNOWax ASTM D6584 EN14105 HP INNUWax GC 2
10. A 01 10 ChemStation B 04 01 2 B100 GC ASTM D6584 EN14105 50 C 2 DB 5ht 3 mL min 50 C 50 C 1 1 15 C min 180 C 0 min 2 7 C min 230 C 0 min 3 30 C min 380 C 10 min FID 380 C 3 GC EN14103 250 C 100 mL min 2 HP INNOWax 1 mL min 210 C 30 FID 250 C GC 2 7693A 7693A
11. 7693A B100 7 B100 FAME GC 2 B100 Agilent 7693A ASTM D6584 EN14105 7693A
12. ww oo co B100 C20 1 7693A B100 5 B100 FAME C17 0 ISTD oo B100 7693A B100 6 B100 FAME a G co gt B100
13. James D McCurry Agilent Technologies Inc 2850 Centerville Road Wilmington DE 19809 USA Agilent 7693A ALS HPI Agilent 7693A ALS 7693A ASTM D6584 EN14105 1 2 FAME EN14103 3 GC
14. 7 30 8 9 800 pL n 10 1 11 10 pL 12 1 uL 13 2 5 5 B100 ASTM D6584 2 5190 1408 5 2 4 10 x 1 mL N N 3x1mL EN14105 5190 1409
15. 3 1 GC 5 ASTM D6584 EN14105 EN14103 EN14110 EN14106 1 5 7890A GC 5188 6576 1 HP INNOWax 30 m x 0 32 mm x 0 25 pm 19091N 113V 2 DB 5ht 15 m x 0 32 mm x 0 1 nm 123 BD11 2 m x 0 53 mm 160 2865 5 FID 2
16. MSTFA 5190 1407 5190 1410 B100 B100 10 mg 2 mL 7693A 1 10 mg B100 2 10 uL 1 3 10 uL 2 4 10 unL MSTFA 5 1 6 30 7 8
17. 0 ASTM D6584 1 Agilent 7693A Agilent 7890A 5 6 2 2 0 0 5 2 je 0 4 Re K 1 5 a D 03 10 _ 0 2 SS y 1 3366x 0 0036 0 5 y 1 7325x 0 1156 0 e RZ 1 000 RZ 0 9936 0 01 02 0 3 04 05 06 0 0 5 1 15 1 0 06 _ 4 8 0 6 s 0 3 i R 04 a R 02 1 a 0 99D0Me000 01 y 10 6531x 0 0337 gt R 1 000 9 RZ 0 9961 0 0 0 0 2 0 4 0 6 0 8 0 0 2 0 4 0 6 0 8 2 Agilent 7693A 5 2 A B100 1 B 7693A B100
18. rs FAME Determination of Free and Total Glycerol and Mono Di and Triglyceride Content European Committee for Standardization Management Centre rue de Stassart 36 B 1050 Brussels 2003 3 EN14103 Fat and Oil Derivatives Fatty Acid Methyl Esters FAME Determination of Ester and Linolenic Acid Methyl Ester Content European Committee for Standardization Management Centre rue de Stassart 36 B 1050 Brussels 2003 www agilent com chem jp www adilent com chem jp Agilent Technologies Inc 2009 Published in Japan April 13 2009 5990 3781JAJP Agilent Technologies
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