Agilent GC/MS によるマグロ中のメチル水銀測定のための同位体希釈法 Manual
Contents
1. eo 15 m 2 1 SERVICE FrontM Equilibration Time lp2 min Fost Run Time Quickcgal Cryo Use Temperature I Timeut Detection min I Fault Detecion 2 we 9A Cancel Post Run En Kk Help EE GC Edit Parameters Dven Temperature 151 0 C 9B GC Edit Parameters Apply ULI Aglent 19091 42. 7890A GC 7688B ALS 5975C MSD HP 5ms 15mx 0 25mmx0 25lum 190918 431 2 CFT 2 way G3181 60500 SilTite CFT GC G2855 60140 0 G2855 60120 1m 0 25 mm CFT G2855 60570 2 CFT SilTite 1m 0 25mm CFT 3 Y T CET
3. 1 Agilent Technologies 1 4 psi Aux EPC 0 8 2 5mL GC S SL MSD MSD 10 75 psi AuxEPC EPC GC AN 1 10 25mL S SL MSD 17 1 cm 2 psi Quickswap 1 0uickSwap Quick Swap Quick Swap GC MSD MSD GC M
4. CFT 0 32 mm 1 0 25 mm 2 7890A 1 PCM A 2 PCM A MSD Agilent 6890 GC POCOT Agilent GC MS
5. MSD MSD EPC GC GC MS EPC MS
6. 7890A GC RPC CEFT Deans GC CFT 1 QuickSwap 1 31 GC MS 2 1 MSD 2
7. 15 m 1 1 m MSD 2 SilTite SilTite Restek Agilent P N 113450 GC 3 GC MSD SilTite
8. 1m Cantrol Mode KZ on E lx Fow Pressure Average Velocity Holdup Time 2 ml min 9 4657 psi Out Vacuum 9824 cr sec ms 250pms D25 1 2555 min a lritial 0 mm He 45 COven Aux Pressure 1 NZ Aux Pressure 2 NZ Aux Pressure 3 NZ FCM A 1 NZ PCM A amp 2 N2 Apply 1 30 m 5A Cancel Rate mLjmin per min Initial Walue mLjmin Help Final yalue will be extended by GC run Hme Post Runi 2 ml min EE GC Edit Parameters Dven Temperalure 45 0 C Description a _ Agllent 190915 433 325 C 30 m Soniolnode On x 250 um x 0 25 pm Flow 25 ml min lritial 0 mm In Front SS Inlet He He 45 Cyen Outi Vacuum C Pressure k 7419 psi DE Average Velocity 48 Cm ec 15ms25Hams025 Haldup Time 0 43433 min Aux Pressure 1 NZ Rate mLimin per min Walue Aux Pressure 2 NZ mLjmin Aux Pressure 3 NZ tinitial FCM A 1 NZ PCM amp 2 N2 Final value will be extended by GC run time Post Runi 25 mL min Apnly Cancel Help
9. CFT OFT DDT CFT 8 4 SIM RTIC 1 2 SIM SIM Scan 13 CFT 10 1 2 DDT 4 CFT
10. 10 1 9C 1 2 15 m 2 9 00 9 50 10 00 10 50 11 00 11 50 12 00 a b F FT IE ps cs Gr ia ip 9 00 9 50 10 00 10 50 11 00 11 50 12 00 la asa ae T FT T TT fT T 9 00 9 50 10 00 10 50 11 00 11 50 12 00 10 6 RTIC 3 4 10 1 RTIC a 15 m 1
11. Mi ee PD 1 03mL 2 4mL 9C 2 I i GC Edit Parameters Dven Temperature 185 3 C O10 IZ oven Temp On 1 0 26 15 m 0 4 1 2 4 15 m 5 10 3 GOC MSD
12. CFT COFT 15 m HP 5ms CFT MSD 15 m HP 5ms CFT CFT GC 1m 15 m HP 5ms SilTite COFT CFT 2 CFT 7890A Advanced User Guide G3430 90015
13. USEPA 8081 44 DDT DDT DDD DDE CFT K WW 6 00 8 00 10 00 12 00 14 00 16 00 18 00 20 00 22 00 24 00 18 30 18 50 1870 18 90 ck Ww RK a Eh ey 6 00 8 00 10 00 12 00 14 00 16 00 18 00 20 00 22 00 24 00 CFT FAME BRTIC m z 74 REIC
14. CFT 15 m 1 BTO CFT 2 7 1 m 1 1 MSD 2 3 GC GC 1 30mx
15. 2 15 m 1 CFT 2 15 m 15 m 2 2
16. 46 2 DDD DDT CFT DDT DDE 2 CFT DDD K amp KR DDE EK EA 20 00 20 20 20 40 20 60 20 80 21 00 21 20 21 40 21 60 21 80 22 00 22 20 22 40 22 60 22 80 44 DDT K EK Dp RK DDD EAY DDE emrlionus CT ES ES ET hE FE i i i ER EL EE FE Ca TE EE I CF ER CES EE CE Ea ES EC Fe CE i a EE EE I i CS Ct i CE RR CE 20 00 20 20 20 40 20 60 20 80 21 00 21 20 21 40 21 60 21 80 22 00 22 20 22 40 22 60 22 80 8 CFT A CEFT 0 2ng DDT GC MS SIM REIC 4 4 DDE DD
17. CFT 1 10m CFT 20 m 30 m Purged Ultimate Union QuickSwap 10 15 m 2 MSD 2 10 10
18. GC CFT EPC IGNORE READY TRUE not ready www agilent com chem jp 1 Agilent 5975C GC MSD 5989 7827JAJP 2 Frank David and Matthew S Klee 5989 6460JAJP 3 Frank David and Matthew S Klee GC MS Analysis of PCBs im Waste Oil Using the Backflush Capability of Agilent QuickSwap Accessory Agilent Technolo gies Dublication 5989 7601EN www agilent com chem jp Bruce Quimby W es Norman Matthew Klee GC MSD CFT Purged Ultimate Union W es Norman wwwagilent com
19. PCT QuickSwap REI OI M S 7890A GC 4 15 m HP 5ms 0 25mm x 0 25um 5976C MSD EI 15 m HP 5ms 0 25mm x 0 25nm 2 GC MSD GC MSD
20. b 2 4mL MSD 4 mL 2 3 CFT CFT 2 way G3180 615
21. 5B 2 15 m 6 2 15 m OFT CFT 30 m SIM 85 1pg uL OFN Ss N CFT 1 Ng 30 m R ThrFPmh rh len trerrriainhrt htt Philr
22. 0 25mmx0 25um 15mL MSD 2 15mx 0 25mmx0 25mum 15 mL MSD 12 mL MSD MSD 7 z 28 GC Edit Parameters 4A 4B 7890A GC
23. 30 m MSD 25psi 055 0 75 50 mL 2 15 mL lt 0 75 4B 120C 15 mL Ix Oven Temperature 45 0 C 3 4 fl M DO lg A We 1 SSL Front ssL Back Spnlit Sp Iless Inlet Gas Saveri 1Y On Heater soc _ h 5 mL min After E min Pressure B4657 Psi Total Flow
24. chem jp Agilent Technologies Inc 2008 Printed in Japan June 24 2008 5989 8664JAJP Agilent Technologies
25. 00 QuickSwap MSD 11 Purged Ultimate Union CFT 11 Purged Ultimate Union G3186 60580 GC DDT Purged Ultimate Union POM EPC 2
26. 31 325 C 15 mx 250 pm x 0 25 pm In Back SS Inlet He Out Wacuum hux Pressure 1 N2 Aux Pressure 2 NZ Aux Pressure 3 NZ2 PCM A 1 N2 PCM A 2 N2 Cancel i Control Mode Flow Pressure Average velocity Holdup Time iF on 2 ml min 3 4557 psi 3 824 cm sec h 2555 min lritial 0 min He 45 C Oven ut Vacuum 3Hmx25 pmx0 25 pm Rate mLjmmin per min Hold Time Run Time value min min mLjmin Help 1 Final yalue will be extended by GC run tirne Post Runi lp3 mL min Dven Temperalure 45 0 C 9C Apply Description Agilent 190915 433 325 C 30 m x 250 pm x 0 25 pm In Fronkt 55 Inlet He Out Vacuum Aux Pressure 1 N2 Aux Pressure 2 N2 Aux Pressure 3 NZ PCM A 1 N2 PCM A 2 N2 1 Control Mode on Flow 25 mL min Inial 0 min He 45 C Oven 7 Pressure zi dpsi DEV RUN Average velocity 48 Cm sec 15mx25mmxH25 Holdup Time 0 43493 mn Rate mLimin per min gt mntaD mm Hold Time Value min mLjmin Help Final value will be extended by GC run time PostRun mmn lx cre
27. 54 2 m min Septum Purge Flow B mL mm Septum Purge Flow Mode standard Made Pused Spitiess a psi until lps min Purge Flovs to Split Vnt mL min at fh min 2 Apply OK 4A Cancel Hep EE GC Edit Parameters Hyen Temperature 450 Split SpIless Inlet I Pressure Total Flow Septum Purge Flow Septum Purge Flow Made Standard mm Gas Saver on f 5 ml min after R min Mode Spiit hd Split Ratio fzs _ f 5 525 ml min OK 4B Cancel Help 5A 5B 2 1 20mL GC Edit Parameters Oven Temperature 45 2 C ngilent 190911 931 325 C 15 mx 250 pm x 0 25 pm In Back 55 Inlet He Out Vacuum 1 25mL
28. E 4 4 DDD DDD EA EK B 2 0ng 4 4 DDT REIC CFT 5 4 4 DDT 6 DDE 7 DDMU CET 9A 9B 9C GOC 338 NR
29. GC MS ee e q Qe W Harry Prest Agilent Technologies Inc 5301 Stevens Creek Blvd Santa Clara CA 95051 USA GC MSD MSD MSD MSD
30. S Quick Swap CFT CFT 15 m CFT 2 Aux EPC 1 GC MSD 1 2 POT QuickSwap MSD MSD 1
31. nlnlrrlnnwrimienWalhtWh Phihrlrrtrltttrltttthtrttrnhehrtlhrihtl 5 00 5 05 5 10 5 15 5 20 5 25 5 30 5 35 5 40 5 45 5 50 5 55 5 60 5 65 5 70 5 75 5 80 5 85 6 CFT 30 m SIM BRTIC 3 lx CFT 1 FAME FAME GC MS 7 CFT CFT
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