Agilent SPME-GC/MS による水質規制農薬 analysis の検討 Manual
Contents
1. W KO KA amp Y NN 6 9 NO SS lt C A 250 200 150 100 50 Polyacrylate 0 0 DVB PDMS NN NN NN 2 KN ER 0 Vw RR CO QO S 9 8 RSy 9 amp R SW amp NR S YA NN KN RS N 9 9 8 Y KN S e O RF S lt Y RA RA2 9 Q KN Ry Ra 4 N Fig 4 SPME 80 30 100ng 1 GCMS 201110NK 002 192 8510 9 1 www agilent com chem jp i Agilent Technologies2. 30 30 ON GC 5 2 ii 250C HP 5msi 30m 0 25mm 0 25um 70C Qnmin 250 m 150 C Omin 9 min 200 C Omin 8C min 280 10min ch1orpyrifos methy 16 593min 280 C MS 70eV 230C SIM 3 SPME Agilent Technologies Polyacrylate 0 5 309 FHig 1 9 100ng 1 30 9 6 Diazinon oxon Malaoxon Isoxathion oxon DVB PDMS KN ww 9
3. a o ee 3 1 SPME GC MS gt SPME GC MS 80 SPME Polyacrylate DVB PDMS 30 100ng 1 100ppt CL ey Words SPME GC MS 1 SPME SPME 7 DVB CAR OS ON 6 SPME GC MS 80 2 Gerstel MPS2 Agilent 7890A 5975C TAD SPME SPME Polyacrylate DVB PDMS 15m1 4 5gs 20ml SPME
4. NaCI 0 NaCI 5 NaCI 30 Fig 1 SPME Polyacrylate 100ng 1 Fig 2 9 30 Polyacrylate DVB PDMS 100ng 1 DVB PDMS 8 Fenitrothion oxon Fig 3 80 30 Polyacrylate DVB PDMS SIM 100ng 1 80 100ng 1 Polyacrylate 72 DVB PDMS 73 80 100ng 1 Polyacrylate DVB PDMS 1 Fig 4 SPME Trichlorfon Dimethoate cc olyacrylate 5 Dichlobenil ccc LO I Ll M MMUA 1 Polyacrylate WE PH ni 2 A Ss 90 ooo s oo Pe s tit Dr
5. TT IMM oo PDVB PDMS ll 1 ll Nl pan NI LA 15oo WU MM JWN ln Polyacrylate Fig S SPME 80 m DVB PDMS SIM 30 100ng 1 4 Polyacrylate 30 6 9 30 Polyacrylate DVB PDMS 30 306 100ng 1 100ppt 80 Polyacrylate 72 DVB PDMS 73 25 0 20 0 15 0 10 0 5 0 Bd ld LL os Na i No m polyacrylate DVB PDMS Q N NN 2 lt Me Q RR QE 1 KS 2 amp KN RS amp 8 amp PA NR SS S 0 WW O NN 8 0 0 NN O Y O N O O O KN N Y N amp K 8
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