Agilent 7696Aサンプル前処理ワークベンチを用いた鉱油 analysis のための Automatic クリーンアップ Manual
Contents
1. Florisil Florisil 140 C Florisil 20 mg 30 mg 2 mg Florisil 200 uL GC FID 150 uL 500 uL 350 150 pL 4 1mlL EPIA Florisil 30 mg LLE 2 mL 1 5 mL2. Agilent Technologies Inc 2011 Printed in Japan October 11 2011 5990 9163JAJP Agilent Technologies
3. ITM GC 1 International standard IS0 9377 2 Water Ouality Determination of hydrocarbon oil index part 2 Method using solvent extraction and as chromatography 2000 F David K Jacq and R L Firor Agilent LTM II Low Thermal Mass 9 2011 59909104JAJP wwwragilent com chem jp www agilent com chem jp
4. d SPE GC FID 10 30 m 30 LTM 2 Agilent 7696 LLE 1 1 5 mL N Florisil
5. 1 Sample 500 uL Dry 2 Dry 1 2 000 pm 4 1 3 Dry 350 pL Clean up Florisil 4 Clean up 1 2 000 rpm 4 1 5 Clean up 150 pL Final GC FID 6 Final Agilent 7890 GC GC SSL LTM I FID 0 32 mm x 10 m 0 10 um DB 5HT 123 5701LTM 1
6. 2 3 5 95 80 lt lt 110 3 n 10 _ 83420 895 4 1 9760 9 206 1045 23 2 97454 206 104 3 23 3 9602 1 197 1028 22 4 9839 3 164 1053 18 5 98418 230 1053 26 6 97045 18 1 103 9 20 7 98004 166 104 9 18 8 97454 230 104 3 26 9 97356 196 104 2 22 10 96584 316 1034 35 97434 209 104 3 23 754 08 RSD 077 077 Agilent 7696A GC FID
7. GC FID HOI TPH 36 C 69 C LLE Florisil N Kuderna Danish GC FID 1 d SPE d SPE LLE
8. Frank David Karine Jacd Bart Tienpont Research Institute for Chromatography President Kennedypark 26 B 8500 Kortrijk Belgium Peter Mrozinski Agilent Technologies Inc 2850 Centerville Road Wilmington DE 19808 USA Agilent 7696A Florisil GC FID Agilent 7696A GC FID LTM GC Agilent Technologies
9. LTM GC FID 1 1 5 000 ug mL cat no 31630 Restek C10 C40 nn 50 ug mL cat no 31678 Restek cat no 31860 Restek IS0 9377 2 000 ng mL n 5 ng uL 80 ng uL 400 ng uL 80 ng uL 2
10. Dry 1 5 mL Florisil 30 mg 2 mg Clean up 1 5 mL Sample 20 mg Dry Florisil 30 mg Clean up 200 pL Final 500 pL 250 uuL 7696 1 Dry Clean up Final ee em Add 1 Agilent 7696
11. 5 5 ng mL 80 ug mL 6 Agilent 7696 2 4 n RSD 1 C40 2 5 80 1 9 n 6 5 2 n n 6 RSD SD C10 58 1 0 542 093 99 6 C20 62 7 0 612 097 99 8 C30 60 4 0 656 1 09 101 1 16 0 2792 175 1 9 C40 50 5 1 293 2 56 86 4 7500000 05 MIN OIL_NO FLORISIL_2 D FID1B ch ST Ry 7000000 1 6500000 6000000 4 55000
12. 2 mL 200 pL Sample Dry Clean up Final 2 2 mL 1 2 Na S0 3 Florisil 4 3 400 ug mL 80 ng mL C38 3 3
13. 2 1 1 0 4 350 C 5183 4647 9 mL min GC 340 C LTM 40 C 0 5 min 200 C min 240 C 100 C min 340 C 0 5 min 3 FID 340 C H 40 mL min 400 mL min 50 mL 900 mL Zymark TurboVap 1 2 mL 2 mL 7696 Agilent 7696 2
14. 1 n 50 ug 800 ng 2 4 000 ug 800 ug 900 mL 50 mL TurboVap 10 mL 100 10 mL 7696 ACS cat no 23 931 3 Sigma Aldrich Florisil cat no 03286 100G F Fluka Sigma Aldrich Na S0 Florisil 140 C 20 mg 2 mg 1 5 mL
15. 00 5000000 4500000 4000000 3500000 1 3000000 2500000 2000000 3 1500000 1000000 500000 1 0 Es 2 60 _ 50000o 06 MIN OIL_3DNFID1B ch amp 6500000 6000000 5500000 5000000 4500000 4000000 3500000 3000000 2500000 2000000 1500000 1 1000000 4 500000 1 0 0 80 1 00 1 20 r T FT 1 40 1 60 1 80 2 00 2 20 2 40 2 60 3 400 ng uL 80 ng uL GC FID Agilent 7696 400 ng mL 80 ng mL 3 RSD lt 1
Download Pdf Manuals
Related Search