Agilent 1H/19F AutoX Triple Resonance Indirect Detection Probe handbook
Contents
1. T T T j T T T T T T T T T T T T T T T T T T T 140 30 140 25 140 20 140 15 140 10 140 05 ppm 140 30 140 25 140 20 140 15 140 10 140 05 ppm Figure 2 Figure 4 Purity analysis P of a sample labeled CF CH 0 P 31P 1H The resulting 10 line pattern indicates nine coupled 9F atoms ta a E O IOM O 140 30 140 25 140 20 140 15 140 10 140 05 ppm 140 30 140 25 140 20 140 15 140 10 140 05 ppm Figure 3 Figure 5 31P 19F The resulting 7 line pattern indicates six coupled H atoms 31P 1H 19F There are two pairs of 3C satellites in the baseline arising from two distinct 13C sites Final Determined Structures Major CF CH 0 P Minor CF CH 0 PO CF4CH 0 P H O CF CH OH www agilent com Ordering Information 1H frequency 500 MHz part number 600 MHz part number Product specifications and descriptions in this document are subject to change without 5 0 mm 199005092 S199006088 notice Agilent Technologies Inc 2011 Published in USA March 3 2011 Publication Number SI 1252 Agg Agilent Technologies2. cee o Agilent H F AutoX Triple a Resonance Indirect Detection Probe Figure 1 Network analyzer plot of simultaneously tuned H F circuit as viewed from single probe port Data Sheet K ey Benefits Performance his probe delivers high sensitivity and outstanding resolution for double and triple resonance experiments involving H 19F and X N 9 P The inner coil is simultaneously double tuned for optimal H F sensitivity and experimental versatility Ease of Use The H 9F AutoX Triple Resonance Probe together with the dual high band configuration of the Agilent NMR System and the ProTune Accessory enables automatic switching of detection and decoupling nuclei Patented probe circuitry and the elegant VNMRS RF routing system eliminate the need to manually move cables or filters Versatility The probe offers simultaneous triple resonance H 19F and X capabil ity The X channel can be tuned over the range of N to P NMR experiments including H 9F F H 19F X HEX X 12F X 1H 1H 19FX 19F 1H X and X H 9F can all be performed effortlessly with the ProTune equipped dual high band configuration of the Agilent NMR System Bee Agilent Technologies 600 MHz Results y Y UV T T T T T I T T T T I T T T T T T T T T T T T T T T T T T T T T T T T T T T
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Agilent 1H/19F AutoX Triple Resonance Indirect Detection Probe handbook