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Agilent 5975C Series GC/MSD handbook

1. Analysis of interest lon 277 00 lon 277 00 Degradation production gw 247 00 Degradation production j 11 60 11 80 12 00 12 20 12 40 12 60 12 80 13 00 13 20 13 40 14 60 13 80 14 00 14 20 14 40 11 60 11 80 12 00 12 20 12 40 12 60 1280 13 00 13 20 13 40 14 60 13 80 14 00 14 20 14 40 Mass chromatograms for the pesticide Fenitrothion acquired via the inert source left and a standard source design right The black line Trace lon Detection delivers a real performance improvement for complex matrices Revolutionary Trace lon Detection technology lets you lower your Method Detection Limit MDL as well as your limit of quantitation LOQ It reduces false negatives and further enhances the per formance of the inert ion source at trace levels The technology also ensures more reproducible baselines dramatically reducing the number of manual interventions during peak integration Trace lon Detection technology gives you a better spectral fidelity increasing your confidence level in the results when doing library matching Time 23 014 23 108 cos a a s Time 22 981 23 083 23 185 23 287 23 389 23 491 23 594 23 696 23 798 23 900 24 002 24 104 Analysis of Fenamiphos Without Trace lon Detection enabled top the compound of interest was missed Trace lon Detection is activated bottom revealing a clear hit for Fenamiphos indicates the ion abundance of the molecular ion of Fenitrothion m z 277
2. dye Jachnolog 10S 59750 inert Xt MSD The Agilent 5975C Series GC MSD Performance productivity and confidence Our measure is your success Agilent Technologies The Agilent 5975C Series GC MSD Proven performance superior productivity and maximum confidence in your results Welcome to the next generation of the industry proven Agilent 5975C Series GC MSD the most popular GC MS of all time The Agilent 5975C inert GC MSD combines innovative design features to boost your lab s productivity and advanced analytical capabilities that help you achieve better results faster Perfectly complemented by the new 890A GC the platform delivers all the elements for perfect chemistry superior performance unmatched reliability greater productivity and enhanced ease of use The Agilent 5975C Series GC MSD is built on a solid foundation of industry leadership reliability and performance tt 2 To learn more about the Agilent 5975C Series GC MSD visit www agilent com chem 5975C Or call toll free 800 227 9770 U S and Canada Gold quartz quadrupole with proprietary design Enhances both performance and reliability up to 1050 u covering all applications from routine El to more demanding CI analyses Page 4 Advanced Analysis Capabilities gt 1050 u mass range a Extends system performance for all models and delivers superior performance for even the most demanding high mass applications industry s lowest mas
3. Thoughtful real world engineering features allow faster easier TL ee ee l HoT Electron impact El ionization with standard Cl ion l l iii S pS LL source Auto CI feature makes Cl as easy as El H ie automated sequence routine maintenance and new self diagnostic and preventive maintenance software makes it easier than ever to keep your lab up and running at peak performance all the time Page 7 New hydrogen El signal to noise specification Permits faster analysis under safe conditions with no compromise on analytical quality Page 7 GC MS software Fits your workflow and your application powerful features and advanced functionality enhance your lab s performance and productivity Page 10 Deconvolution Reporting Software Gives you fast answers with the confidence you need together with new Retention Time Locking databases DRS significantly reduces post run analysis time Page 12 GC MS columns and supplies High performance Agilent J amp W GC columns and supplies meet every analytical need Page 15 Engineering that s all about performance and productivity At Agilent building the world s most trusted GC MS The submicron layered gold hyperbolic electrode surfaces give solutions is an ongoing challenge anda process of continual maximum transmission while maintaining resolution across the full improvement With each new generation of instruments mass range up to 1050 u Bak
4. clean and virtually maintenance free Agilent is the first mass spectrometer manufacturer to offer this unique pump which requires virtually no routine maintenance There s no oil and no danger of oil contamination or leaking Designed for supportability and maintenance Agilent GC MSD systems have always been designed for easy serviceability and maintenance and the Agilent QuickSwap Capillary Flow device saves time and 5975C Series GC MSD takes this design philosophy to money with every column change and system a whole new level maintenance To purge gas line Lock nut To MSD ma transfer line To EPC To column Tired of waiting around for a mass spec to vent before you can change a column out or perform routine inlet maintenance Using a QuickSwap Capillary Flow device you can safely disconnect the column without venting and without losing vacuum in about 30 seconds e Modular analyzer assembly offers complete access to the filament ion source mass analyzer and electron multiplier for ele aE OI pact faster routine maintenance n fact the entire analyzer assembly can be removed in less than two minutes without tools A modular self contained electronics module minimizes problems POSE TO packilush at 0min with cables and wiring harnesses Front glass window provides simple source identification as Original well as a complete view of critical connections so you can see for sure the col
5. 35 00 40 00 reduces data review time from hours of tedious work to Surface Water Sample 2 minutes of unattended computer analysis The DRS software automates the following operations e Quantitation by target compound analysis software on 5 00 10 00 15 00 20 00 25 00 30 00 35 00 40 00 e Spectral Deconvolution or cleaning of full scan spectra f p 9 p Total lon Chromatogram of typical surface water extracts Library searching of cleaned spectra Data courtesy of the California Department of Food and Agriculture The revolutionary solution combines three different software packages e Agilent s GC MSD ChemStation e The National Institute of Standards and Technology NIST Mass spectral Search Program with the NIST MS Library e NIST s Automated Mass Spectral Deconvolution and Identification Software AMDIS Three new database libraries Comparison of the time to process 17 surface water samples e Hazar hemical Compounds RTL Database for rapid and K ooun pi 7 compot us P CDFA A skilled analyst processing the 17 samples took about accurate identification of chemical agents 8 hours to review results and eliminate false positives Agilent DRS Fully automated process took about 30 minutes e Pesticide and Endocrine Disruptor RTL Database for rapid is and found an additional 99 compounds and accurate quantitation of these agents in large numbers of samples e Indoor Air Toxics RTL Library for identification
6. 5989 6105EN
7. Data Analysis tools allow you to analyze files simultaneously Enhanced flexibility features e Simple standard reports or easily customizable reports let you best meet your lab s needs A variety of reports may also be easily exported to XLS HTML or XML formats e Advanced macro programming provides additional capability for customization e Integrated control of PAL autosamplers enables automated large volume sample injection Available option e Deconvolution Reporting Software DRS combined with appli cation specific Retention Time Locked Libraries reduces hours of manual data review to only minutes of automated processing Available option e Integration with Agilent OL Enterprise Content Manager ECM makes it easy to store retrieve and organize GC MS methods data and reports 10 To learn more about the Agilent 5975C Series GC MSD visit www agilent com chem 5975C Or call toll free 800 227 9770 U S and Canada SemiQuant Quickly and easily estimate the concentration of non calibrated compounds Agilent s SemiQuant capability works together with Retention Time Locking RIL databases to increase confidence in your compound identification and speed up the quantification process When an unknown peak appears a library search provides only a possible match with the sample spectrum Using the appropriate RTL database you can increase certainty by matching the reten tion time of your compound with a fixed ret
8. based motadata values gt To search for multiple words you may use AND and OR between seaech terms gt To search for a phrase enclose it in quotation marks gt The or X characters can be used as a wikicard characters To search for these chatacters tethun bad Ley must be preceded rih a Y character e g or Ve gt Number and Date Tame values can be reached unng Smart end Advanced Search gt Orly the keywords related to the latest revinon are searched Agilent OL Enterprise Content Manager ECM is a web based application that provides a secure centralized repository for all of the electronic data generated in your organization Comprehensive search and collaboration tools allow users to effectively find use and re use the information they need to make intelli gent business decisions Agilent OL ECM makes your lab more efficient productive and confident by enabling the collection and conversion of the broadest range of analytical data into accurate and actionable information Rapid Deconvolution Identification and Quantification in Complex Matrices Agilent s simple easy to use Deconvolution Reporting Surface Water Sample 1 Software DRS is an optional software feature that saves hours of analysis and review The best deconvolution soft ware in the industry the software quickly finds compounds that traditional data analysis packages miss In fact it LATTI ey 5 00 10 00 15 00 20 00 25 00 30 00
9. promised In fact our GC and GC MS instrument specifications are determined using industry leading Agilent J amp W columns and Agilent brand chromatography supplies Eliminate concerns about lost samples or productivity from unexpected sequence interruptions by using Agilent certified autosampler vials septa and caps and Gold Standard syringes Each comes with a Certificate of Conformance to assure you all specifications are met Agilent J amp W GC columns and our portfolio of chromatographic supplies are available through Agilent and authorized Agilent distributors Agilent services let you focus on what you do best Agilent s service organization is the most respected in the industry Whether you need support for a single instrument or a multi laboratory operation we can help you solve problems quickly increase your uptime and optimize your lab s resources We offer e On site preventive maintenance to ensure dependable operation and minimize unplanned downtime e Troubleshooting maintenance and repair for Agilent as well as non Agilent instruments e Remote diagnostic and monitoring services to maximize instrument uptime and lab productivity e Industry leading regulatory compliance services and education e Expert consulting and training e Cooperative support for in house service organizations The Agilent Value Promise 10 years of guaranteed value In addition to continually evolving products we offer something el
10. Series The new Agilent 7890A Gas Chromatograph brings Important new separation capabilities and productivity features to the industry leading Agilent GC platform lt ee t i z mm T Agilent Performance and Reliability Expanded Chromatographic Capabilities 5th generation electronic pneumatics control EPC and digital Highly flexible EPC design enables even more sophisticated electronics set a new benchmark for retention time locking RTL hydrocarbon analyses An optional 3 detector TCD can speed precision and retention time repeatability and help make the up complex gas analyses and allows more types of analyses to 7890A Agilent s most dependable GC ever be run ona single GC Higher Productivity Easier Operation Faster oven cool down robust backflush capability advanced Practical time saving design features speed up and simplify automation features and faster GC MS oven ramps let you get routine maintenance more done in less time at the lowest possible cost per sample all easily incorporated into your existing methods 8 To learn more about the Agilent 5975C Series GC MSD visit www agilent com chem 5975C Or call toll free 800 227 9770 U S and Canada The Agilent 7890A GC works right into your current 6890 workflow with no major changes to your methods You can increase your productivity and take advantage of the new capabilities of the 7890A system with no disrupt
11. and quantitation of toxics in the workplace 12 To learn more about the Agilent 5975C Series GC MSD visit www agilent com chem 5975C Or call toll free 800 227 9770 U S and Canada Accessories and options make your 5975C even more versatile and productive Automatic Liquid Samplers pertect productivity partners for your 5975C Series GC MSD Add an Agilent 7683 Series Automatic Liquid Sampler Offering the fastest injection times of any GC autosampler greater solvent capacity multiple sampling options dual simultaneous injection certified autosampler vials and more the 683 ALS Is ready to go to work Boost your lab s output with automated sample preparation Choose the versatile CombiPAL sample injector for liquid injection headspace and solid phase microextraction SPME The economi cal GC PAL platform can be contigured for liquid injection only but offers many of the other capabilities of the CombiPAL including large volume injection LVI multiple vial and syringe sizes and extended sample vial capacity yo oot 2 see Ges 4 Agilent Technologies G1888 a Network Hea ee Agilent G1888A Headspace Sampler adds to your analysis capabilities Automatically introduce volatile compounds from virtually any sample matrix directly into a GC or GC MS An inert sample pathway from vial through column to source provides superior chemical performance without analyte degradation or loss Oil free pump
12. ate results every time for El PCI and NCI modes e Retention Time Locking RIL gives you repeatable retention times across systems regardless of operator detector type and column maintenance In combination with Agilent or user created databases it will let you quickly screen unknown peaks with added confidence e Synchronous SIM Scan and AutoSIM automatically and easily convert any full scan method to a high sensitivity SIM or SIM Scan method enabling you to acquire both SIM and Scan data in a single run e eMethods functionality allows you to efficiently share and distribute methods across multiple laboratories or to save development time by downloading application methods from the Agilent Website e SemiQuant estimates the concentration of uncalibrated compounds that may be of potential importance e Data reprocessing lets you reprocess a previously run sequence while new data are being collected e Enhanced Data analysis and Easy EIC tools expand your system s qualitative analysis capabilities sa Enhanced Data Analysis Analyze Multiple Data File Eile Chromatograms Spectrum Library Structure DataBase Tools Macros View Help to 118 70 O02cw002 d data ms to 140 70 Of2eu002 didata ms i ain 1 unda lon 118 00 117 70 to 118 70 O04co004 d data ms fon 14000 139 70 to 140 70 OD4co004 d data ms lon 118 00 117 70 to 118 70 005c0005 d data ms lon 140 00 133 70 to 140 70 O05co005 d data ms The enhanced
13. aving to constantly recontigure Methane Is used to optimize the ion source and perform the mass calibration a separate inlet port is provided for a second reagent gas including ammonia An intuitive software user interface and a Cl flow control module work together to automatically adjust the Cl reagent gas flow for optimum Cl performance 149 DI n octyl phthalate 0 I SG oon Oo OS CH3 0 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Dioctyl Phthalate El Mass spectrum obtained using CI source in automated sequence Abundance Average of 7 744 to 7 764 min phth 10 ng PCINH3 1 D data ms ws PCI NH Abundance w NCI NH an at aided biel biel Mil bhi biel ie abel Mild rer fr r m z gt 80100 120 140 160 180 200 220 240 260 280 300 320 340 360 30 440 420 m z gt 80 100 120 140 160 180 200 220 240 260 280 300 320 340 340 380 409420 Abundance Scan 865 7 756 min phth 10 ng NCICH4 1B D data ms W NCI CH 600 M 390 250 148 N F a peter roe eer robe T Time off set for clarity m z gt 80100120 140 160 180 200 220 240 260 280 300 320 340 340 380 409 420 Diocty phthalate in all CI modes Many compounds yield little identifying information in El for example all phthalates look very similar CI provides valuable additional spectral infor mation PCI with ammonia upper left PCI with methane lower left NCI with methane lower right and NCI with a
14. b s performance productivity and confidence Performance Choose Agilent J amp W columns and supplies for a leak free inert flow path to ensure lowest bleed and best signal to noise per formance in Agilent GC MSD systems From among the full suite of Agilent low bleed J amp W columns the inert HP OMSi column was selected to ship with the new 5975C Specially tested to ensure maximum area response performance of strong acid and base compounds this column is also compatible with Agilent Pesticide Libraries for MS Tight inlet seals are needed to keep MS system performance at Its peak Agilent liners pre cleaned and conditioned liner O rings matched with our new proprietary injection molded gold plated seal prevent the tiniest leaks that cause column bleed and signal deterioration Productivity Agilent supplies help keep routine maintenance routine Our capil lary column ferrules O rings and septa are packaged to not only remain clean and ready for use but to conveniently dispense one at a time as needed for fast inlet maintenance An exclusive non stick plasma coating on our premium inlet septa and pre cleaned O rings makes maintenance quicker and easier no unscheduled inlet maintenance due to residue on the inlet surface and shorter bakeout times after preventive maintenance so you can start running samples sooner Confidence Agilent J amp W columns and supplies ensure your Agilent 5975C sys tem delivers as
15. e 20x more Peaks of interest elute by 16 minutes but a 24 minute bake out at 320 C is required to elute heavy compo nents Using the 7890A system s backflush capability the sample was rerun with a 4 minute backflush saving 20 minutes per run 50 total cycle time savings ALS Overlap and faster cool down save an additional 4 minutes per cycle The Agilent 6850 Series I GC The Agilent 6850 Series GC small rugged easy to use Is your lab doing simple routine applications or at line analysis The Agilent 6850 GC combined with the 5975C VL GC MSD is the perfect choice if you need just a single inlet and detector The small footprint system offers a surprising number of advanced features as well as legendary Agilent reliability ooo d GC MS software that fits your workflow and your application perfectly The Agilent MSD Productivity ChemStation makes it easy even for non expert operators to take advantage of all the advanced capabilities of the Agilent 5975C inert GC MSD system You ll find everything designed to help you make the most of every run and every workday The MSD ChemStation software includes four industry focused packages Enhanced Mode EnviroQuant DrugQuant and Aromatics in Gasoline Unique productivity features e Control of two GC MS systems from a single MSD ChemStation via built in LAN communication saves time resources and bench space e Automatic tuning ensures more accur
16. ention time in addition to spectral data Should you wish to quantify the compound semiQuant helps by estimating the concentration so that you can inject the appropriate level of the standard Quantitation Report Not Reviewed Data Path C msdchem 1 data Data File evaldemo d z 7 Sep 1989 13 59 D Peterson demoscan sample 16 ng per component ALS Vial 1 Sample Multiplier 1 Quant Time Mar 18 15 39 59 2666 Quant Method msdchem 1 HETHODS EVALDEMO SQ UN M Quant Title Semi quant tests QLast Update Thu Mar 09 13 51 45 2006 Response via Initial Calibration Internal Standards R T Qlon Response Conc Units Dev Hin gt 1 Dodecane 5 286 57 9737444 Target Compounds 2 Biphenyl 6 4391 154 27583844 1666 66 ng 3 4 Chloroabiphenyl 7 741 188 18794921 1666 66 ng SemiQuant compounds are highlighted at the bottom of the Quantitation Report eMethods Replicate share and distribute methods With Agilent eMethods recreating and replicating a new GC MS method is now a quick and fully automated process You can bring a new GC MS online in the shortest possible time and maximize lab productivity by standardizing on methods whether your instruments are across the hall or across the world Integration with Agilent OL Enterprise Content Manager ECM streamlines data handling and organization Ta RITU F EJ mpane p QC0POPEE z gt zz Use Quick Seaech tn find fles based on thel inst
17. eout to 200 C enables more robust determinations as well as outstanding high mass stability and minimal we never lose sight of our goal to help your lab get better g ig y maintenance An available high mass checkout kit provides added results with higher confidence and process more samples l confidence that high mass is accurately reported in the shortest possible time 799 The gold standard in quadrupole design and performance The quadrupole used in the Agilent 5975C Series GC MSD a incorporates a combination of patented proprietary Agilent 400 299 technologies to deliver superior performance and significantly 207 enhanced reliability 458 639 721 320 533 959 361 266 480 561 690 611 1 881 425 510 589 663 751776 821850 909932 997 m z 200 250 300 350 400 450 500 550 600 650 700 750 800 850 900 950 1000 Analysis of Decabromodipheny ether PBDE 209 demonstrates exceptional high mass detection capability 959 m z High sensitivity AutoTune makes it easy to optimize system performance Take the trial and error out of optimizing operating conditions by automating the process The 59 5C system s AutoTune feature saves time boosts performance and Improves instrument to instrument consistency The true hyperbolic quartz structure offers extremely low thermal n expansion and exhibits excellent dimensional stability The unique design results in lower field errors versus rou
18. ion to your lab s smooth operation Right out of the box operators will be right at home with the familiar controls and user interface and because the 7890A system is built upon proven 6890 GC inlets detectors and GC oven you can transfer methods to your new 890A GC with complete confidence Breakthrough Capillary Flow Technology Agilent s innovative Capillary Flow modules enable reliable leak free in oven connections Available in a number of useful configu low dead volume devices not only make it easy to make secure connections they give you the ability to precisely divert your gas flow where and when you want This opens the door to highly useful tech niques such as flow splitting backflushing and Deans Switching that can improve your analytical results as well as saving time and resources Perform SSL inlet maintenance in seconds Convenient new Turn lop design is built into each split splitless SSL inlet allowing you to change liners and columns more quickly and easily than ever betore without special tools or training rations these inert low mass 7890A GC gives you a net improvement in productivity 5000 ppm oil 4 min backflush of spike 20 min saved Solvent blank after backflush sensitive inlet and column clean than above NOI ANNATA EPA 8270 5 ppm EPA 8270 standard run spiked into 5000 ppm of a heavy oil to simulate interference from a hazardous waste Scal
19. m s synchronous SIM Scan operation OA you can get both in a single run Even better you don t have to More Signal be a GC MS expert to do it Agilent s AutoSIM software capability automatically converts full scan data into SIM or SIM Scan acquisi Pr tion parameters for use in synchronous SIM Scan methods SIM dwell times can be set in 1 msec increments from over 100 msec to as low as 1 msec dwell time 7 60 7 62 7 64 7 66 7 68 Chlorothalonil More signal Total ion chromatogram of Heptachlorobiphenyl compares standard electronics Agilent 5973 Series MSD to new fast electronics Both chromatograms were acquired by the same instrument at the same scan speeds horizontal offset for clarity Time 1460 1465 1470 1475 1480 1485 1490 1495 1500 No sensitivity loss in SIM The overlay above compares SIM only acquisition blue to the SIM signal from a synchronous SIM Scan acquisition red 6 To learn more about the Agilent 5975C Series GC MSD visit www agilent com chem 5975C Or call toll free 800 227 9770 U S and Canada Cl as easy as El Chemical lonization Cl has long been considered an advanced GC MS technique because of complex setups reagent gas adjust ment and ion source tuning Now the Agilent 5975C inert GC MSD makes Cl as routine and easy as El without sacrificing the spectral information of El The dual inlet port configuration allows you to operate your Cl system at optimum performance levels without h
20. mmonia upper right Notice the differences in spectra and total response shown at center Average of 7 756 to 7 776 min phth 10 ng PCINH3 1 D data ms Use hydrogen to lower your cost per analysis The new hydrogen signal to noise specification for the 5975C Series GC MSD makes Agilent the first and only instrument manufacturer to certify the perform ance and safety of hydrogen as a carrier gas In fact hydrogen often can provide faster analysis times with no compromise of analytical quality Analysis of polyaromatic hydrocarbons using He and Hz In this example H2 actually provides better resolution An upgrade can give new life to your older instruments If your lab has a 5973 GC MSD here s some good news your instrument can be upgraded to high performance SIM Scan capability In fact most of the new features presented in this brochure are available for older instruments through upgrades that enable you to take advantage of the latest technology The Agilent 7890A Gas Chromatograph The next level of GC performance and productivity Adding an exciting new chapter to a 40 year history of GC leadership Agilent s new 7890A flagship GC gives you everything you need to take your lab to the next level of GC MS performance including advanced chromatographic capabilities powerful new productivity features and real time self monitoring instrument intelligence Plus of course legendary Agilent reliability 76820
21. nd rod quadrupoles as well as excellent resolution and mass axis stability regardless of ATUNE U 400V laboratory temperature fluctuations User selectable AutoTune settings make it easy to set the right operating parameters every time 4 To learn more about the Agilent 5975C Series GC MSD visit www agilent com chem 5975C Or call toll free 800 227 9770 U S and Canada Solid inert ion source up to 350 C boosts your system performance Agilent s proprietary inert source is now programmable up to 350 C to provide enhanced response for active compounds and late eluters including pesticides It delivers exceptional electron impact ionization and lets you run sample after sample with complete confidence The source is constructed of a solid inert material so there is no inert coating that can wear away over tine and which can ultimately compromise your data The inert ion source eliminates surface activity reactions for more reliable library matches It also requires less frequent cleaning improving your lab s productivity Later eluter Methoxychlor 6 00 Enhanced Analysis for Organochlorine Pesticide shows dramatic improve ment for the later eluting compounds Agilent s 350 C inert ion source increases sensitivity in all modes El PCI and NCI A net improvement in peak shape can as well be observed in NCI mode Abundance Inert source Standard source amp Analysis of interest
22. s deviation ensures longer lasting tuning and This powerful combination provides better MS resolution and the calibration Page 4 The modular mass analyzer incorporates a proprietary quartz quadrupole a solid inert ion source and industry leading detector lowest mass deviation available it also assures superior sensitivity 350 C inert ion source Now programmable up to 350 C delivers enhanced response for active compounds and late eluters Page 5 and spectral integrity tor the highest confidence in your results New Trace lon Detection technology provides even more capabilities at trace level Higher Throughput Lowers detection limits in complex matrices I together with the high temperature inert ion mos Le We A eae source this new technology gives your lab detection cycle times enable you to process more samples with aas E Eee i gt powerful new analytical capabilities Page 5 Trace lon Detection technology Comprehensive automation features and faster separation and more confidence Advanced analysis routines let you get more information from every run and automated spectral deconvolution identification and quantification software simplifies post run analysis Maximum Uptime Synchronous SIM Scan mode Lets you selectively monitor for ions of interest at high sensitivity while simultaneously acquiring library searchable scan data Page 6 All tonization modes in one
23. se unique to the industry our 10 year value guarantee The Agilent Value Promise guarantees you at least 10 years of instrument use from your date of purchase or we will credit you with the residual value of that system toward an upgraded model Not only does Agilent ensure a safe purchase now we help ensure your investment is as valuable to you in the long run e o 0 ee e J j Agilent Technologies The Agilent Service Guarantee Should your Agilent instrument require service while covered by an Agilent service agreement we guaran tee repair or we will replace your instrument for free No other manufacturer or service provider offers this level of com mitment to keeping your laboratory running at maximum productivity For more information Learn more www agilent com chem 59 5C Buy online www agilent com chem store Find an Agilent customer center in your country www agilent com chem contactus U S and Canada 1 800 227 9770 agilent_inquiries agilent com Europe info_agilent agilent com Asia Pacific adinquiry_aplsca agilent com Research use only Information descriptions and specifications in this publication are subject to change without notice Agilent Technologies shall not be liable for errors contained herein or for incidental or conse quential damages in connection with the furnishing performance or use of this material Agilent Technologies Inc 2007 Printed in USA March 16 2007
24. the green line is attributed to a low concentration degradation product m z 247 yy Powerful analytical capabilities improve results and productivity Fast electronics enhance performance and enable synchronous SIM Scan Fast electronics used in the 5975C Series GC MSD maxi mizes signal transmission for fast GC MS in full scan and Selected lon Monitoring SIM modes It also enables syn chronous SIM Scan functionality without compromising analytical performance 760 762 764 7 66 768 7 60 7 62 7 64 7 66 768 770 Fast GC MS in SIM Fast electronics capture more data points for improved integration of narrow peaks giving you more accurate sensitive and reproducible quantitation High Performance Selected lon Monitoring SIM b be hathah and Full Scan Agilent s synchronous SIM Scan functionality lets you capture SIM data and full scan data in the same acquisition Because of the ease of setup and availability of spectral libraries many labs use full scan for most of their data collection SIM mode on the other 7 55 7 60 7 65 710 eT or hand offers a significant improvement in sensitivity over full scan More data points 50 full scan data points across 0 84 sec peak measured i at half height Data acquired at 10 000 u sec half height data however SIM data cannot be searched against commercially available spectral libraries for match confirmation Performance Electronics 6 250 u sec Now with the 5975C syste
25. umn iS connected properly 5 00 10 00 15 00 20 00 25 00 30 00 3500 40 00 e High reliability vacuum system assures maximum long term The Quickswap device can also be used for column backflushing performance available oil free pumping system virtually eliminates reducing MSD contamination by high boiling sample components pump maintenance and reduces noise and can be used with shortening analysis time and increasing the lifetime of your ion corrosive gases such as ammonia SOUICE Off axis high energy dynode HED detector delivers long life and superior sensitivity New Electron Multiplier Saver feature further extends system service duty cycle e Optional ion gauge helps to troubleshoot and isolate leaks as quickly as possible 14 To learn more about the Agilent 5975C Series GC MSD visit www agilent com chem 5975C Or call toll free 800 227 9770 U S and Canada High performance Agilent J amp W columns and supplies for the Agilent 5975C Series GC MSD To help you achieve better results faster Agilent is continu ously improving the cleanliness convenience and reliability of columns and supplies for Agilent GC MSD systems From market leading J amp W columns with rigorous quality control and QC testing that ensure reproducibility efficiency and inertness to GC flow path supplies designed manu factured and packaged to maintain the integrity of your sample Agilent columns supplies and accessories will improve your la

Agilent 5975C Series GC/MSD handbook

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